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Position the kettle so that the center bottle of the kettle is sitting on a submersible stirrer. Units used in 21 CFR This standard is also available to be included in Standards Subscriptions. It is applicable to resins containing greater than 0.
The following explanations of r and R It is applicable to resins containing greater than 0. This document asgm not an ASTM standard and is intended only to provide the user of an ASTM standard an indication of what changes have been made to the previous version.
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ASTM D5227 – 13
This test method provides a means to determine the amount of hexane-soluble low molecular weight material present in polyolefins. The methods presented apply to post-consumer plastics. Please first log in with a verified email before subscribing to alerts.
The FDA protocol also states the temperature of the contents must be brought to Reagents and Materials 7.
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ASTM D – 13 – Standard Test Method for Measurement of Hexane Extractable Content of Polyolefins
Need more than one copy? This standard is not included in any packages. NOTE 34—Care must be exercised when cutting the samples to avoid ragged edges on the specimen. Historical Version s – view previous versions of standard. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Replace the kettle head with condenser column. Because it may not be technically possible to adequately depict all changes accurately, ASTM recommends that users consult prior editions as appropriate. This test method is based upon the presumption that the weight of the residue extract present in the solvent is equal to the amount extracted from the film sample and could therefore be quantified by measuring the weight loss of the extracted film, eliminating the complex and time-consuming evaporation process described in 21 CFR Techniques to separate and identify incompatible plastics, moisture, chemicals, or original product residues, and solid contaminants such as metals, paper, glass, and wood are essential to the processing of recycled plastic materials.
Note 1—There is no known ISO equivalent to this standard. If the temperature exceeds these limits, the test must be discontinued and restarted.
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Referenced Documents purchase separately The documents listed below are referenced within the subject standard but are not provided as part of the standard. Add to Alert PDF. An American National Standard Designation: This section may also include descriptions of the changes or reasons for the changes, or both. Precision and Bias 12 We have no amendments or corrections for this standard. Recycled plastic materials may contain incompatible plastic or other undesirable contaminants that could affect the processing or quality, or both, of the plastic prepared for reuse.
ASTM International takes no position respecting the validity of any patent rights asserted in connection with any item mentioned in this standard. Start stirring and allow the hexane to heat for 1 h. Where no current ASTM standard exists, however, this guide gives procedures for the separation or identification, or both, of specific contaminants.
Work Item s – proposed revisions of this standard. Note 1 — There is no known ISO equivalent to this standard. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. Historical Version s – view previous versions of standard. Subscription pricing is determined by: Users of this standard are expressly advised that determination of the validity of any such patent rights, and the risk of infringement of such rights, are entirely their own responsibility.
Current edition approved June 15, It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Link to Active This link will always route to the current Active version of the standard. This edition includes revisions to Section 10, Calculation. Summary of Test Method 4. Appendix X1 lists the tests and the specific contaminant addressed by each procedure. Extract for 2 h. A superscript epsilon indicates an editorial change since the last revision or reapproval.